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The resulting combination was vigorously mixed to produce a diluted hydrophobic premix wherein mixing was achieved under conditions of standard temperature and pressure.

Physico-chemical Data.

IL. L. LLL. LLLLLL.

AEROSIL R is a fumed silica aftertreated with organosilane (HMDS) with high specific surface and marked hydrophobia.

AEROSIL R S fumed silica after treated with HMDS based on AEROSIL It is used in paints and coatings, adhesives and sealants, and silicone.

Company The Evonik Coating Additives Business Line from Evonik offers its customers with optimal solutions in the paints, coatings and printing ink sectors and supports them with the production of resource-efficient coatings.

In a most preferred embodiment of the invention the composition does not form a permanent coating on application and is preferably free from varnish.

Viscosity of fluids such as silicone oils can be determined, for example, by the relevant international standard, such as ISO Also for the avoidance of doubt and by way of illustration in this specification, a composition with microclusters comprising silica-based particles yields support for a composition with microclusters consisting essentially of and consisting of silica-based particles.

None of the efforts set forth above describes a composition for making a superhydrophobic coating generated from a composition comprising aggregates or microdusters of silica-based particles, silicone and solvent wherein the aggregates or microdusters have a diameter from 1 nm to nm and the silicone has a viscosity of at least 30 cSt.

A process for making the composition of as claimed in any one of the preceding claims, comprising the step of combining, in no particular order, aerosl silica-based particles, at least a first part of the solvent and the silicone to provide a mixture.

Additionally or alternatively the coating may display a sliding angle for water of less than 15 degrees or even from 0.

SEM images of these films showed a smooth and compact surface and so hydrophobicity of the film is mainly attributed to low surface energy of silicone.

The composition as claimed in claim 1 or claim 2, wherein the silica-based particles are hydrophobically-modified fumed silica particles.

Super-hydrophobic coating material, preparation method thereof and super-hydrophobic coating.

A further advantage of silicones employed in the present invention is that they typically have a refractive index which is close to that of 8r12 particles.

The present inventors have recognized that there is a need to generate coatings that do not alter the look of surfaces they are applied on.

Advantageously polar organic solvent may be r182 to improve the compatibility of silicone with water.

This example demonstrates superhydrophobic films made from dispersions wherein the solvent comprises water.

The average size z-average of the aggregates in the dispersion containing silicone was nm whilst for the dispersion without silicone the size was nm.

In particular it is preferred that where the silica-based particles have a refractive index n pthe silicone has a refractive index n s and the ratio np n s of n p to n s is within the range 0.

Typically, the hard surface is in a household including window, kitchen, bathroom, toilet, furniture, floor, or the like.

Disclosed is a composition capable of yielding a superhydrophobic coating.

Additionally or alternatively, the ratio np n a of n p to n a is within the range 0.

Where a feature is disclosed with respect to a particular aspect of the invention for example a composition of the inventionsuch disclosure is also to be considered to apply to any other aspect of the invention for example a method of the invention mutatis mutandis.

This example demonstrates the effect of the arosil of surface modification of fumed silica particles on film properties.